- Rinse the burette with the standard solution, the pipette with the unknown solution, and the conical flask with distilled water.
- Place an accurately measured volume of the analyte into the Erlenmeyer flask using the pipette, along with a few drops of indicator. Place the standardized solution into the burette, and indicate its initial volume in a lab notebook. At this stage, we want a rough estimate of the amount of known solution necessary to neutralize the unknown solution. Let the solution out of the burette until the indicator changes color, and record the value on the burette. This is the first titration and it is not very precise; it should be excluded from any calculations.
- Perform at least three more titrations, this time more accurately, taking into account where the end point will roughly occur. Record the initial and final readings on the burette, prior to starting the titration and at the end point, respectively. (Subtracting the initial volume from the final volume will yield the amount of titrant used to reach the endpoint.)
- The end point is reached when the indicator permanently changes color.